北京市场调味品中防腐剂和甜味剂使用状况调查与分析
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宋书锋 男 助理研究员 研究方向为食品理化分析 E-mail:songshufeng_1977@126.com

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TS202

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Investigation and analysis on preservatives and sweeteners in condiments in Beijing market
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    摘要:

    目的 了解调味品中防腐剂和甜味剂的使用状况,为添加剂的风险评估提供依据。方法 将样品均质、酸化后,用乙醚提取,氮气吹干后用流动相定容,过微孔滤膜后进高效液相色谱仪分析,以甲醇+0.02mol/L乙酸铵(12+88,体积比)为流动相,使用DiamonsilTMC18 柱,在波长230mm进行检测,流速为0.8ml/min。结果 苯甲酸、山梨酸、糖精钠和安赛蜜检出率分别为28.3%、20.4%、18.6%和23.9%,没有检测结果超标。结论 北京市场的调味品中添加剂的使用符合《食品添加剂使用卫生标准》,相对以往国家监测而言更加安全,但酱油中防腐剂和甜味剂的检出率和最大检测值在调查的4类调味品中相对较高,应加强监测。

    Abstract:

    Objective To learn about the status of preservatives and sweeteners in condiments and to provide a basis for risk assessment on food additives. Methods After the samples were homogenized, acidified, extracted by ether and then dried with nitrogen, the residues were dissolved with the mobile phase and made to a certain volume. After filtered by a 0.45μm films, the test solutions were injected onto a DiamonsilTMC18 column of HPLC, and then eluted by methanol-ammonium acetate (12+88, V/V) at the flow rate of 0.8ml/min, and detected at the wavelength of 230nm. Results The detection rate of benzoic acid, sorbic acid, sodium saccharin and acesulfame potassium were 36.9%, 17.9%, 15.5% and 26.2%, respectively. No result was out of the limit of the national standard. Conclusion The use of food additives in condiments in Beijing market was conformed to the hygienic standards. Comparison with the results of national surveillance, the content of preservatives and sweeteners in condiments in this study was safer. The detection rate and maximum value in sauce were higher than that in other condiments, the surveillance on preservatives and sweeteners in sauce should be strengthened.

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宋书锋,张烁,杨大进,刘艳君.北京市场调味品中防腐剂和甜味剂使用状况调查与分析[J].中国食品卫生杂志,2011,23(3):270-272.

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  • 收稿日期:2010-07-28
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