比较测量法同时测定食品中总α总β放射性
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(南通市疾病预防控制中心,江苏 南通 226007)

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顾俊 男 主任技师 研究方向为卫生理化检验E-mail:gujun502@163.com通信作者:何智敏 女 副主任医师 研究方向为环境卫生E-mail:hzmntcdc@126.com

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Determination of gross alpha radioactivity and gross beta radioactivity in food at the same time through comparative measurement method
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(Nantong Center for Disease Control and Prevention,Jiangsu Nantong 226007,China)

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    摘要:

    目的 建立能同时测定食品中总α、总β放射性的方法。方法 样品经干燥、炭化、灰化后制成样品源,放入低本底α、β测定系统中同时测定样品总α、总β计数率,并与标准源测定效率比较定量。结果 总α放射性测定探测限在0.160~5.31 Bq/kg(鲜重),加标回收率在82.7%~101.8%之间,相对标准偏差(RSD)在5.65%~7.26%(n=5)之间;总β放射性测定探测限在0.475~9.29 Bq/kg(鲜重),加标回收率在88.8%~114.8%之间,RSD在2.23%~9.19%(n=5)之间。结论 本方法实现了食品中总α、总β放射性的同时测定,简便、高效,适用于批量食品样品的总放射性监测。

    Abstract:

    Objective A method was developed for measuring gross alpha radioactivity and gross beta radioactivity at the same time in food. Methods Sample was prepared after drying, coking, ashing, and the counting rate of gross alpha and beta in sample was measured through the low background alpha and beta measurement system, and quantitative comparison was made with the standard source measurement efficiency. Results The detection limit of gross alpha was 0.160-5.31 Bq/kg (fresh weight). The recovery was 82.7%-101.8%. RSD was 5.65%-7.26% (n=5). The detection limit of gross beta was 0.475-9.29 Bq/kg (fresh weight). The recovery was 88.8%-114.8%. RSD was 2.23%-9.19% (n=5). Conclusion This method could determine the gross alpha radioactivity and gross beta radioactivity in food at the same time, simply, efficiently, and is suitable for total radiation monitoring of the batch food sample.

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顾俊,何智敏,叶青华,张卫兵.比较测量法同时测定食品中总α总β放射性[J].中国食品卫生杂志,2018,30(1):46-49.

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  • 收稿日期:2017-07-05
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  • 在线发布日期: 2018-04-02
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