油炸和膨化食品中氯丙醇酯及缩水甘油酯污染调查研究
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作者单位:

唐山市疾病预防控制中心,河北 唐山 063000

作者简介:

杨秋月 女 副主任检验技师 研究方向为食品污染物监测 E-mail:yue13323296615@163.com

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R155

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Contamination analysis of chloropropanol esters and glycidyl esters in fried food and puffed food
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Tangshan Center for Disease Control and Prevention, Hebei Tangshan 063000, China

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    摘要:

    目的 调查油炸及膨化食品中3-氯-1,2-丙二醇酯(3-MCPDE)和2-氯-1,3-丙二醇酯(2-MCPDE)和缩水甘油酯(GE)的污染状况,为油炸及膨化食品中MCPDE和GE的风险评估提供数据参考。方法 建立油炸和膨化食品中氯丙醇酯及GE同位素稀释气相色谱-串联质谱法,对55份油炸食品和66份膨化食品进行定量检测及污染水平分析。结果 油炸和膨化食品中3-MCPDE、2-MCPDE和GE检出率均为100%,油炸食品中3-MCPDE、2-MCPDE和GE含量范围分别为0.052 5~1.59、0.023 2~0.798和0.025 7~3.06 mg/kg。膨化食品中3-MCPDE、2-MCPDE和GE含量范围为0.089 2~2.31、0.047 7~0.867和0.075 5~2.58 mg/kg。结论 MCPDE和GE含量水平均呈现膨化食品高于油炸食品的趋势,对膨化食品中MCPDE和GE的污染需要优先关注。

    Abstract:

    Objective To analyze the contamination levels of 3-MCPDE (3-monochloropropane-1,2-diol esters), 2-MCPDE (2-monochloropropane-1,3-diol esters) in fried food and puffed food, and we could provide a scientific basis for conducting risk assessment to the exposure levels of MCPDE and GE.Methods We detected chloropropanol esters and glycidyl esters by isotope dilution gas chromatography - tandem mass spectrometry and conducted an analysis of 3-MCPDE, 2-MCPDE and GE contamination levels in 55 fried food samples and 66 puffed food samples.Results The detection rates of 3-MCPDE, 2-MCPDE and GE in fried food and puffed food were all 100%, and the concent range of 3-MCPDE, 2-MCPDE and GE in fried food were 0.052 5-1.59, 0.023 2-0.798 and 0.025 7-3.06 mg/kg. The concent range of 3-MCPDE, 2-MCPDE and GE in puffed food were 0.089 2-2.31, 0.047 7-0.867 and 0.075 5-2.58 mg/kg.Conclusion The results indicated that the contamination levels of 3-MCPDE, 2-MCPDE and GE in puffed food were higher than fried food, and we should put more attention on MCPDE and GE contamination in puffed food.

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杨秋月,孙仕萍,陈琪,王佳宝.油炸和膨化食品中氯丙醇酯及缩水甘油酯污染调查研究[J].中国食品卫生杂志,2025,37(3):252-257.

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  • 收稿日期:2025-02-10
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  • 在线发布日期: 2025-06-25
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